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85 个结果
  • 简介:本文通过高分辨X射线衍射及掠入射(GID)的实验方法对生长在SrTiO3衬底上的LLa2/3Ca1/3MnO3和YBaCu3O7单层膜及YBa2Cu3O7-x/La2/3Ca1/3MnO3异质结构双层薄膜的微结构进行了研究。结果发现,所有薄膜都呈c向生长。由于热膨胀系数的不同而引起的热应力使得LCMO膜的晶格参数与靶材的相差较大。La2/3Ca1/3MnO3在单层腹及双层膜中都由靶材的立方结构变成了薄膜状态的四方结构。YBa2Cu3O7在单层膜及双层膜中都由靶材的正交结构变成了薄膜状态的四方结构。La2/3Ca1/3MnO3膜与YBa2Cu3O7膜在不同的样品中处于不同的应力状态。

  • 标签: YBa2Cu3O7-x/La2/3Ca1/3MnO3 异质结构薄膜 微结构 X射线衍射 X射线掠入射 锰酸盐
  • 简介:LiGaO2与GaN的晶格失配率只有0.2%,是一很有潜力的蓝光衬底材料。本文利用化学侵蚀、光学显微镜、透射电子显微镜对晶体中的缺陷进行了分析,研究了生长参数、原料化学配比对晶体质量的影响及其和晶体中缺陷形成的关系。TEM分析表明,由于原料近非化学计量比挥发致使组份偏离,容易产生γ-Ga2O3包裹物。包裹物和位错形成具有一定的相互促进作用。X射线貌相分析发现提拉法生长LiGaO2晶体中易于形成平行于(001)面的亚晶界,这可能和其沿[001]方向的极性有关。

  • 标签: GAN 外延衬底材料 LiGaO2晶体 X射线貌相术 氮化镓 TEM
  • 简介:ThispaperpresentsabriefoverviewofCO2reformingofCH4(CRM)byvariousformsof'arc'plasma,whichismoresuitabletoCRM,andtheenergyefficiencyisusedtoevaluatedifferentplasmaprocessesspecifically.Accordingtothereportedresults,thearcthermalplasmawithbinodeexhibitedbetterperformance.Moreover,theplasmaCRMprocesswascomparedwiththereportedplasmasteamreformingofCH4(SRM)process,andtheresultsshowedthattheformerprocesshasadvantagesonenergyefficiencyandCH4consumption.Additionally,itisbelievedthattheplasmaCRMprocesswouldbecompetitivewiththeconventionalSRMprocessinbothenergyefficiencyandCO2emissiononcetheheatmanagementisemphasizedandtherenewablepowerisused.Finally,aconceptofplasmareactorforindustrialapplicationisproposed.

  • 标签: 等离子体过程 CO2排放 蒸汽重整 CH4 可再生能源发电 等离子体反应器
  • 简介:PhotocatalystwaspreparedbyimmobilizingTiO_2onglassbeadsusingthetradi-tionalsol-gelmethod.Ultravioletlight(UV)producedbypulsedstreamerdischargewasthenusedtoinducephotocatalyticactivityofTiO_2photocatalyst.Decolourationefficiencyoftherep-resentativeazodye(acidorange7,AO7)wasinvestigatedusingthesynergisticsystemofpulsedstreamerdischargeplasmaandTiO_2photocatalysis.Theobtainedresultsshowedthatthede-colourationrateofAO7couldbeincreasedby16.7%undertheconditionofaddingsupportedTiO_2inthepulsedstreamerdischargesystem,comparedtothatinthesolepulsedstreamerdischargeplasmasystem,duetothesynergisticeffectofpulsedstreamerdischargeandTiO_2photocatalysisinducedbypulsedstreamerdischarge.ThesynergisticsystemofpulsedstreamerdischargeandTiO~photocatalystwasfoundtohavemorereactiveradicalsfordegradationoforganiccompoundsinwater.

  • 标签: 脉冲海洋地震拖缆放电 固体二氧化钛 光催化作用 增效系统
  • 简介:Theoreticalcalculationandexperimentalresultsforapolarizerwithsinusoidalgroovesusedintheelectroncyclotronresonanceheating(ECRH)systemoftheHL-2Atokamakarepresented.Thecalculationisbasedonanintegralmethoddevelopedinthevectortheoryofdiffractiongratings,andthepolarizationcharacteristicsobtainedwithalow-powertestareingoodagreementwiththenumericalcalculatedresults.WiththepolarizerassembledinamiterbendintheECRHtransmissionline,pureordinarymode(O-mode)andextraordinarymode(X-mode)polarizedwavesarealsoexpectedinthehigh-powerexperiment,dependingonthepolarizerrotationangleandthetoroidalinjectionangleoftheelectroncyclotron(EC)wavebeam.Second-harmonicX-modeexperimentsweresuccessfullyexploredinHL-2A.Experimentalresultrevealedthattheelectrontemperatureincreasedfrom0.8keV(Ohmicheatingphase)to1.5keV(secondX-modeheatingphase).

  • 标签: 电子回旋共振加热 偏光镜 采暖系统 正弦 HL 装置
  • 简介:GaAs半导体材料可以提高器件运行速度,日益引起人们的注意,但是也给器件制造者带来了许多问题。在本文个,一个全新的可应用于HEMT器件的深亚微米X射线T栅工艺被提出来,该工艺采用三层胶方法,曝光实验是在北京同步辐射3BlA束线上进行的,并且取得了好的结果。

  • 标签: GAAS 半导体材料 亚微米X射线T型栅工艺 制造 半导体器件 X射线光刻
  • 简介:Thepreliminarydesignofamulti-barrelspelletinjectorwithcyclerefrigeratorasanadvancedplasma-fuellingtoolforHL-2Atokamakhasbeenproposed.Thedesignaimsatprecisetemperaturecontrol,easyoperation.withhighreliabilityandhighflexibility.GM-cyclerefrigeratorandpipe-gunStructurehavebeenemployedtoproduce25pelletsin25gunbarrelssimultaneouslyandthedesignaims.havebeenaccomplished.Primedesignprinciple,engineeringparameters,structureandlayoutofthecryostatcomponentsaswellascalculationofheatloadforthecryostatarepresented.

  • 标签: 托卡马克装置 球形注射器 循环制冷 热量损失 散热片
  • 简介:TheprecisionofplasmaelectrondensityandFaradayrotationanglemeasurementisakeyindicatorforfar-infraredlaserinterferometer/polarimeterplasmadiagnosis.Toimprovetheprecision,anewmulti-channelhighsignal-to-noiseratioHCOOHinterferometer/polarimeterhasbeendevelopedontheHL-2Atokamak.Ithasahigherlevelrequirementforphasedemodulationprecision.Thispaperintroducesanimprovedreal-timefastFouriertransformalgorithmbasedonthefieldprogrammablegatearray,whichsignificantlyimprovestheprecision.Wealsoapplyareal-timeerrormonitoringmodule(REMM)andastableerrorinhibitingmodule(SEIM)forprecisioncontroltodealwiththeweaksignal.Wetesttheinterferometer/polarimetersystemwiththisimprovedprecisioncontrolmethodinplasmadischargeexperimentsandsimulationexperiments.Theexperimentalresultsconfirmthattheplasmaelectrondensityprecisionisbetterthan1/3600fringeandtheFaradayrotationanglemeasurementprecisionisbetterthan1/900fringe,whilethetemporalresolutionis80ns.ThisperformancecanfullymeettherequirementsofHL-2A.

  • 标签: HL-2A装置 等离子体诊断 电子密度 转角测量 控制处理 高精度
  • 简介:InHL-2Atokamaks,thebehaviorofheatfluxdepositedonthedivertortargetshasbeenstudiedduringdeuteriumgasfuelling.Theheatfluxisreducedsignificantlyaftersupersonicmolecularbeaminjection(SMBI)fuellingduringOhmicandelectroncyclotronresonanceheating(ECRH)divertordischarges.TheSMBIfuellingcausesanincreaseintheplasmadensityandthischangeresultsintheexperiencedchangeoftheedgeproperties.MostofthisreductionindivertortargetheatfluxoccurstogetherwithahighplasmaradiationregionlocatedatneartheX-point.Thelargestreductioninheatfluxprofilesisobservedattheoutboarddivertorseparatrixstrikepoint,whiletheheatfluxfarfromthestrikepointremainsalmostunchanged.Inparticular,withSMBImulti-pulsesgasfuelling,apartiallydetacheddivertorregimeisobservedwithahighlyradiatingregionattheX-point.Withtheonsetofthepartiallydetacheddivertorregime,asuddendropinbothheatfluxandpowerflowonthedivertortargetisobserved.Thereductioninpowerloadonthedivertortargetsisroughlyequaltotheincreaseinplasmaradiationloss.

  • 标签: 偏滤器靶板 HL-2A装置 热通量 红外热像 HL-2A托卡马克 等离子体密度
  • 简介:Theγ-Fe2O3nanoparticlescoatedwithDBSandCTABwerepreparedbythemicroemulsionmethod.Thecoatedsamplesshowenhancednonlinearopticalpropertiescomparedwiththeirbulkcouterpart.The.Moessbauerspectraatroomtemperatureweremeasuredforthecoatedferricoxides.Themonolayersoftheorganicmoleculearefoundtohaveastrongchemicalbondwiththesurfaceatomsandthushaveasignificantinfluenceontheelectronstructureofparticlesurface.@1999ActaMetallurgicaInc.

  • 标签: 氧化铁 纳米粒子结构 表面活化剂 DBS CTAB
  • 简介:TheNi-AlalloycontainingCr,FeadditiveswerepreparedasRaneyNiCatalystbyhighenergymilling.ThesizeandsurfacestateofNi-Alalloypowderwerestudiedbyparticlesizeanalyzerandsanningelectronmicroscopy.theStructurewasanalyzedbyXRDandMoessbauermethods.Theresultsshowedthatafterahigh-energymilling(HEM).theNi-Alalloytransformstoanano-scaleNiAlstructurewithrichAl.Byannealingthealloy,ametastableNi2Al3phasecanbeobtained.

  • 标签: 催化剂 催化剂镍 纳米晶体
  • 简介:ThetransientopticalpropertiesofnovelPbSnanoparticlescoatedwith2.6-O-diallyl-β-cyclodextrines(CDs)werestudiedbythefemtosecondpump-probetechnique.Theresultsshowthattheultrafasttransient-inducedabsorptionforthenovelcase.ComparedtothePbSnanoparticlesstabilizedwithpolyvinylalcohol(PVA),wefindthattheprocessforthenovelcaseisdifferentfromthePbS(PVA),WesuggestthattheCDssurfacemodificationcantrapholesonthesurfaceofPbSnanoparticles.ThiscaninduceanefficientchargeseparationbetweenthePbSnanoparticlesanditssurfaceandresultinanultrsafast-inducedabsorptionfornovelPbSnanoparticles.

  • 标签: PBS 纳米颗粒 表面化学处理 非线性光学特性