简介：Theanalysisofstableisotopesofcarbonandoxygenindifferentcarbonaterocksbythephosphoricacidmethodisnoteasierthanthatbythelasersamplingmethoddevelopedinrecentyears,whichopticallyfocuseslaserbeamswithsufficientenergyonamicroareaofathinsectioninavacuumsampleboxviamicroscope.CO2producedbyheatingdecompositionofcarbonatewaspurifiedbythevacuumsystem,andthestableisotopicvaluesofcarbonandoxygenwerecalculatedandanalyzedonamassspectrometer.Thispaperadoptedthelasermicro-samplingtechniquetoanalyzethestableisotopesofcarbonandoxygenindolomite,carbonatecement,stromatoliteanddifferentformsofdawsonite(donbassite).Resultsindicatedthatthelasermicro-samplingmethodiseffectiveinanalyzingcarbonatecompositionandcouldbeaconvincingproofforjustificationoncarbonatecompositionanalysis.