简介：FifteennewpolyesterligandswerepreparedbycopolymerizationofEDTA(ethylenediaminetertraaceticacid)dianhydrideorDTPA(diethylenetriaminepentaaceticacid)dianhydrideanddihydricalcoholordihydricphenol.Theirparamagneticmetalcomplexeswerealsosynthesized.Allpolyesterligandsandmetalcomplexeswerecharacterizedby^1HNMR,IRspectraandelementalanalyses.Preliminarystudyshowedthatthepolyestermetalcomplexeshadhigherrelaxationeffectivenessascomparedtocorrespondingsmallmolecularmetalcomplexes.

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简介：Objective:Todetectsuperoxideanion(O-2)signalsintheheart,liver,lungandkidneytissuesafterburns.Methods:Twenty-fourmaleratswererandomizedinto4groups.Theratsofexperimentalgroupswereimmersedin100℃waterfor15secondsand25%third-degreeburnwascreated.Thoracotomyorlaparotomywasperformedat5,10,15,20and30minutesafterburn,andspecimensoftheheart,lung,liverkidneywereobtainedforburnedrats.Thespecimenswerethenpreservedinliquidnitrogenforcryo-preservationanddetectedimmediatelyusingEPR.Results:ThesignalsofsuperoxideOradicalappearedintheheart,lung,liverandkidneyspecimens10-15minutesafterburn.Conclusions:Thereisadirectevidenceofoxygenfreeradicals(OFRs)injurytovisceraofburnedratsbetween10-15minutesafterburn.

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